I'm glad that you guys are clear about using 2% H202. I would have
thought more is better too. I finally have some use for that gallon of
32% HCL in the garage.
Mike
--- In Homebrew_PCBs@yahoogroups.com, "fenrir_co" <fenrir@...> wrote:
>
> --- In Homebrew_PCBs@yahoogroups.com, garydeal <garydeal@> wrote:
> >
> >
> > This afternoon I finally got around to mixing up a small batch
> >of
> > the 1/3 HCl + 2/3 H2O2. I've read the positive reviews on that
> >recipe
> > here, but was really surprised/impressed at the results.
> > My usual initial test is to cut a small strip of .005" brass
> >and
> > wave the end around in the solution, and it dissolved in record
> >time. So,
> > I set up a sheet with some photoresist (laminated dry-film), burned
> >my
> > favorite test file into the resist, developed it and popped it into
> >the
> > beaker. I hesitate to say that it took minutes to etch, it would
> >make
> > more sense to describe it as seconds. Since the test file has two
> >parts
> > panels, I dropped the second one in and it was nicely finished in
> >short
> > order. The guy that craves these parts is going to be really
> >pleased, as
> > am I.
> >
> > Question:
> > The solution total was about 225 ml, and the brass sheet was
> >etched
> > one sided with an etch area of a couple of square inches. Afterward
> >the
> > solution was quite hot and bubbling like soda pop on the stove. I
> >put it
> > in a cold water bath to cool it down, but I have to wonder - is
> >there the
> > possibility of a runaway reaction and what is the result?
> >
> > Oh, and I'm sure this is common knowledge to the rest of you,
> >but on
> > say, a 1 oz and 2 oz board, what are the copper thicknesses?
> >
> > Thanks,
> > -Gary
> >
>
> Your mixture is far too strong, you need to add more water (add acid
> to water, not water to acid, though with regular muriatic the danger
> isn't nearly as bad as adding water to lab grade sulfuric acid). The
> 40 volume H2O2 adds some water, but not enough, it seems. You don't
> want the stuff etching so fast that you can't even get it out in time,
> plus the fumes, heat, etc, might melt the container it's in.
>
> Also, you want a bucket with a /lot/ of baking soda dissolved in it to
> neutralize the etchant. During my one trial run with this process, I
> discovered that sharpies and other permanent markers are useless as a
> resist with this process, so you'd need to touch up with tough paint
> on a fine brush. I'm sticking with FeCl3 so that if I /have/ an
> accident I won't burn myself instantly.
>