copper plating
2003-11-17 by roel_cnc
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Index last updated: 2026-03-31 13:47 UTC
Thread
2003-11-17 by roel_cnc
2003-11-18 by Adam Seychell
> Hi,
>
> I'm trying to get me bath plating but it isnt working as it should be!
> only thing i got is a dark brown easely wipe of film
> pcb is 10 sq cm power supply gifs 1,8 volts ad 0,7 amps
> also tryt a 5 volt make same result only faster
> have to tell the bath solution is made as adam's style with a
> terracotta pot - acid is pritty blue
>
> gr. Roel
>
>
>
>
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2003-11-18 by mpdickens
> > I'm trying to get me bath plating but it isnt=====
> working as it should be!
> > only thing i got is a dark brown easely wipe of
> film
2003-11-18 by twb8899
> Hi,be!
>
> I'm trying to get me bath plating but it isnt working as it should
> only thing i got is a dark brown easely wipe of film
> pcb is 10 sq cm power supply gifs 1,8 volts ad 0,7 amps
> also tryt a 5 volt make same result only faster
> have to tell the bath solution is made as adam's style with a
> terracotta pot - acid is pritty blue
>
> gr. Roel
2003-11-18 by twb8899
> Hi,be!
>
> I'm trying to get me bath plating but it isnt working as it should
> only thing i got is a dark brown easely wipe of film
> pcb is 10 sq cm power supply gifs 1,8 volts ad 0,7 amps
> also tryt a 5 volt make same result only faster
> have to tell the bath solution is made as adam's style with a
> terracotta pot - acid is pritty blue
>
> gr. Roel
2003-11-18 by roel_cnc
> Cathode current density (C.D.) normally between 10 ~ 20 mA/sq.cm.YES got real tiny bubbles also if i change amps as u describe it
> Are you getting hydrogen from the PCB ?
> If so then C.D. is too high or copper too low.the copper must be to low then.
> To check approx. copper sulfate concentration make up a testshould be!
> solution of your desired concentration (e.g. 80 g/L CuSO4.5H20)
> and put it in a test tube. Then take sample of plating solution
> and put into a identical test tube and fill to equal height. Look
> though the end of each test tube and compare the color.
> This will get you +-20% accuracy which can be good enough.
>
>
>
> roel_cnc wrote:
> > Hi,
> >
> > I'm trying to get me bath plating but it isnt working as it
> > only thing i got is a dark brown easely wipe of filmfiles:
> > pcb is 10 sq cm power supply gifs 1,8 volts ad 0,7 amps
> > also tryt a 5 volt make same result only faster
> > have to tell the bath solution is made as adam's style with a
> > terracotta pot - acid is pritty blue
> >
> > gr. Roel
> >
> >
> >
> >
> > Be sure to visit the group home and check for new Bookmarks and
> > http://groups.yahoo.com/group/Homebrew_PCBshttp://docs.yahoo.com/info/terms/
> >
> > To unsubscribe from this group, send an email to:
> > Homebrew_PCBs-unsubscribe@yahoogroups.com
> >
> >
> >
> > Your use of Yahoo! Groups is subject to
> >
> >
2003-11-19 by Adam Seychell
> --- In Homebrew_PCBs@yahoogroups.com, Adam SeychellIn that case you plated amorphous copper, which is like copper
> <adam_seychell@y...> wrote:
>
>>Cathode current density (C.D.) normally between 10 ~ 20 mA/sq.cm.
>>Are you getting hydrogen from the PCB ?
>
>
> YES got real tiny bubbles also if i change amps as u describe it
>Also don't forget to keep an eye on the current density !!.
>>If so then C.D. is too high or copper too low.
>
>
> the copper must be to low then.
> can i do the same thing again with the terra cotta pot (if needed)Of course, just put the pot back and continue generating copper
> with the same solution.
>
>>To check approx. copper sulfate concentration make up a test
>>solution of your desired concentration (e.g. 80 g/L CuSO4.5H20)
>>and put it in a test tube. Then take sample of plating solution
>>and put into a identical test tube and fill to equal height. Look
>>though the end of each test tube and compare the color.
>>This will get you +-20% accuracy which can be good enough.
>>
>>
>>
>>roel_cnc wrote:
>>
>>>Hi,
>>>
>>>I'm trying to get me bath plating but it isnt working as it
>
> should be!
>
>>>only thing i got is a dark brown easely wipe of film
>>>pcb is 10 sq cm power supply gifs 1,8 volts ad 0,7 amps
>>>also tryt a 5 volt make same result only faster
>>>have to tell the bath solution is made as adam's style with a
>>>terracotta pot - acid is pritty blue
>>>
>>>gr. Roel
>>>
>>>
>>>
>>>
>>>Be sure to visit the group home and check for new Bookmarks and
>
> files:
>
>>>http://groups.yahoo.com/group/Homebrew_PCBs
>>>
>>>To unsubscribe from this group, send an email to:
>>>Homebrew_PCBs-unsubscribe@yahoogroups.com
>>>
>>>
>>>
>>>Your use of Yahoo! Groups is subject to
>
> http://docs.yahoo.com/info/terms/
>
>>>
>
>
>
> Be sure to visit the group home and check for new Bookmarks and files:
> http://groups.yahoo.com/group/Homebrew_PCBs
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>
>
2003-11-19 by Steve
--- In Homebrew_PCBs@yahoogroups.com, "twb8899" <twb8899@y...> wrote:
...
> A regulated power supply may not be the best way to make a rectifier.
> I have always used a "variac" variable transformer controlled
> rectifier for plating. This allows to current to be set without the
> power supply trying to compensate. The voltage will end up where it
> needs to be if the current is set properly. You could try using a
> model train transformer for your rectifier or use a triac lamp dimmer
> to control the power supply transformer. Maybe some of these ideas
> will help.
2003-11-19 by Stefan Trethan
> Around here, a search of thrift stores turns up quite a few modelI found out that variac transformers are really cheap at ebay.
> train transformers and slot car tranformers, at very cheap prices.
>
> Not all light dimmers will handle a transformer as a load and may blow
> out. If the transformer is at too high a voltage, you can ease both
> problems by putting an incandescent light bulb in series with the
> primary and attach this to the light dimmer.
>
> Steve
2003-11-19 by Stefan Trethan
2003-11-19 by mpdickens
2003-11-19 by pminmo
> Well, it is maybe hard to admit but i am a stupid git.paper ;-)
>
> Toner transfer works MUCH better if you use the right side of the
2003-11-20 by Adam Seychell
> Does anyone on the list have a specific pump
> (Manufacturer and part number) that they can recommend
> for spray etching? It would be most helpful if the
> recommendation was based on personal experience.
>
>
> Best regards
>
>
> Marvin Dickens
> Alpharetta, Georgia USA
>
> =====
> Registered Linux User No. 80253
> If you use linux, get counted at:
> http://www.linuxcounter.org
>
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2003-11-20 by mycroft2152
> Well, it is maybe hard to admit but i am a stupid git.paper ;-)
>
> Toner transfer works MUCH better if you use the right side of the
> .Welcome to the club. I've been using the clay coated paper with good
>
2003-11-20 by mpdickens
> It just so happens my current project is building aObviously, I am also building a spray etcher. I
> spray etcher.
2003-11-20 by Stefan Trethan
2003-11-21 by Adam Seychell
>
> which etchants don't eat up stainless steel?
>
> I know sulphuric acid shouldn't, how about HCl?
>
> thanks
> st
>
>
> Be sure to visit the group home and check for new Bookmarks and files:
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2003-11-21 by mpdickens
> I'm pretty sure ammonium persulfate is ok, but don'tHi Adam,
> take my word
> for it,
2003-11-21 by Adam Seychell
> --- Adam Seychell <adam_seychell@...> wrote:What you describe is similar to my findings. Centrifuge pumps are
>
>>It just so happens my current project is building a
>>spray etcher.
>
>
> Obviously, I am also building a spray etcher. I
> searched through the message archives and I found
> references to a couple of pumps (One was even
> recommended...). However, upon examination of these
> pumps (Using spec sheets published by the manufacturer
> or by talking to manufacturer tech support) it became
> obvious that they were not suitable due to either the
> materials used in thier construction or not enough
> pressure (GPH is never the problem). If anyone bought
> those pumps, the etchant most definately destroyed the
> shafts (Stainless 316) or the impellers (Delrin) or
> both.
>
> I have been looking at centerfuge pumps and diaphram
> pumps (Just as you have). However, I have not looked
> at the Shurflow or flowking lines (Although I'm gonna
> take a look based on your recommendations).
>
> I have found one pump that has suitable materials used
> in the construction and produces the desired pressure.
> However, it's a submersible and I'm not thrilled with
> that (So, I'm not going to purchase it...). It was
> $36.00 USD at my local hardware store.
>
> Well Adam, it looks like you and I are breaking new
> ground (At least for this list).
>
>
2003-11-21 by Leon Heller
----- Original Message -----
From: "Stefan Trethan" <stefan_trethan@...>
To: <homebrew_pcbs@yahoogroups.com>
Sent: Thursday, November 20, 2003 9:18 PM
Subject: Re: [Homebrew_PCBs] Pump for sray etching
>
>
> which etchants don't eat up stainless steel?
>
> I know sulphuric acid shouldn't, how about HCl?
HCl does, judging by what happens to my stainless steel kitchen sink. 8-)
How about a peristaltic pump?
Leon
--
Leon Heller, G1HSM
Email: aqzf13@...
http://www.geocities.com/leon_heller
2003-11-21 by Stefan Trethan
2003-11-21 by Markus Zingg
>Well, if stainless is no good in HCl,Hi Stefan
>which Materials would be good for constructing
>a PCB holder for a vertical etch tank?
>
>
>I think carbon reinforced tubes are very strong. (from rc model supply)
>Does the HCl attack the carbon fibers? I think it should not be
>a problem with epoxy resin (as pcbs are also this material).
>
>
>How to construct a holder?
>It should allow for etching on both sides and the full surface (no clamps
>or such stuff)
>
>
>Any hints appreciated.
>
>thanks
>
>Stefan
2003-11-21 by Marty Grove
2003-11-21 by Stefan Trethan
2003-11-21 by Stefan Trethan
2003-11-21 by mpdickens
> Well, if stainless is no good in HCl,Mine are made of lexan (Lexan which is considerably
> which Materials would be good for constructing
> a PCB holder for a vertical etch tank?
2003-11-21 by Stefan Trethan
>> (this is the rotrary sprayer we discussed before)Tin-plating (optional)
>> (What? tin powder in water? how does this work? really?)st
2003-11-21 by Leon Heller
----- Original Message -----
From: "Stefan Trethan" <stefan_trethan@...>
To: <homebrew_pcbs@yahoogroups.com>
Sent: Friday, November 21, 2003 3:28 PM
Subject: [Homebrew_PCBs] PCB Holder construction and materials
> Well, if stainless is no good in HCl,
> which Materials would be good for constructing
> a PCB holder for a vertical etch tank?
Titanium will probably be OK. Some of the commercial tanks use PVC-coated
steel wire.
Leon Heller, G1HSM
Email: aqzf13@...
http://www.geocities.com/leon_heller
2003-11-22 by mpdickens
> FLFLojetQuad II Diaphragm" 4406 seriesWell, I just purchased a ShShurflo088-422-444 (US
> ShShurfloAqua King Premier" 2088-422-144
2003-11-22 by mpdickens
> FLojet "Quad II Diaphragm" 4406 seriesWell, I just purchased a Shurflo 2088-422-444 (US
> Shurflo "Aqua King Premier" 2088-422-144
2003-11-22 by mpdickens
2003-11-22 by Stefan Trethan
2003-11-23 by Adam Seychell
> I just completed a 45 minute run of the Shurflow
> fitted with the heat exchanger/heat sink. The pump
> worked like a champ and never cut out. Therefore, it's
> safe to say it was worth the extra $ 20 USD. OTOH, if
> I have to run the pump longer than 15 minutes (And at
> 15 minutes we are talking a board with unrealistic
> copper weight), I've done something horribly wrong...
>
> I figure using only 33% of a proven 45 minute run
> gives me pleny of room in the event I do sucessive
> runs back to back.
>
>
> Best regards
>
>
> Marvin Dickens
> Alpharetta, Georgia USA
>
> =====
> Registered Linux User No. 80253
> If you use linux, get counted at:
> http://www.linuxcounter.org
>
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2003-11-23 by Adam Seychell
2003-11-23 by mpdickens
> What was the voltage and current duringI set the pump up in a configuration I was told was
> your test ?
2003-11-23 by Adam Seychell
> --- Adam Seychell <adam_seychell@...> wrote:
>
>
>>What was the voltage and current during
>>your test ?
>
>
> I set the pump up in a configuration I was told was
> the most common in an RV (At least, most RV's here in
> the US):
>
> 12 Volts
> 5.5 AMPS (The pump is rated up to 7.0 amps)
>
> Question:
>
> What are the dimensions and specifications of the
> nozzles that you are using. I've settled on using
> quanitity-6 180 degree fan nozzles (Three for the
> front of a pcb and three for the back of a pcb.
> Further, I think I'm going to use quantity-2,
> windshield wiper motors to rotate the nozzles back and
> forth. This will afford me multiple speeds of 180
> degree back and forth rotation without having to do a
> stepper motor. Also, I've found a portable plastic
> sink that I'm going to use as the enclosure that
> houses the spray machine. I going to build a door that
> fits on the top of the sink that will have a lexan
> window for viewing. The drain in the bottom of the
> sink will be connected to a gasoline can (Firmly
> attached, but quickly and easily removable). The
> etchant will be pumped from the gasoline can into the
> enclosure and then allowed to drain back into a
> gasoline can (For easy maintenace). So, basically,
> during the etching process, the etchant will circulate
> between the gasoline can and the enclosure via the
> pump. Modularizing the etchant allows for a couple of
> features/benefits:
>
> 1.) I can filter the etchant as it etches (Less wear
> on the pump) so that viscosity stays realively
> constant.
>
> 2.) Regenerating etchant and/or changing out etchant
> is easy.
>
> 3.) I can easily wash the pump out with h20 following
> use without diluting/contaiminating the etchant.
>
> 4.) I can wash the board in the machine prior to
> removal.
>
> 5.) breaking down the etching machine is easy: The
> etchant is self contained and easily storable.
>
>
> Best regards
>
>
> Marvin Dickens
>
> =====
> Registered Linux User No. 80253
> If you use linux, get counted at:
> http://www.linuxcounter.org
>
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2003-11-24 by mpdickens
> I mentioned the nozzle types I'm using in one of myI'll look back through my emails.
> earlier replies.
> What you propose sounds interesting.How are you planning on doing it?
> Just a quickcase you end up scraping it and starting again :)
> warning, try not spend a lots of money on an idea in
> I think one of the most difficult tasks building aFunny you say mention this. Ever since I started
> spray etcher is configuring the nozzles and spray
> patters so you get uniform etching. I'm sure the
> spray etching equipment manufactures spent lots on
> R+D to get this right.
2003-11-24 by mpdickens
2003-11-24 by Adam Seychell
> Oh yeah, I forgot to mention that the total estimatedExcellent, Will love to see the finished result. But don't rush
> cost of this device as currently visioned is $110.00
> USD excluding the nozzles, which I think is pretty
> good for a quality spray etcher. But, as with most
> projects, this number could increase by 20% ( And in
> this case, however unlikely, drop by as much as
> 3%...)unless I royally screw the design up.
>
> As soon as this project is complete, tested and
> working, I'll post pictures, a bill of materials and a
> few notes.
>
2003-11-26 by mpdickens