Plated Thru Hole at Home
2002-02-27 by j_hallows
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2002-02-27 by j_hallows
2002-03-01 by JanRwl@AOL.COM
> Other than using eyelets has anyone made Plated Thru Hole at Home andDITTO! I have OFTEN needed "onesy-twosey" PCB's with PTH, and have had to
> can give some tips?
2002-03-01 by Dwayne Reid
>In a message dated 27-Feb-02 10:42:43 Central Standard Time,I use 2 methods:
>j_hallows@... writes:
>
>
> > Other than using eyelets has anyone made Plated Thru Hole at Home and
> > can give some tips?
2002-03-01 by j_hallows
> each! Seems plating-through should be within the realm of us ol'steps,
> home-brewers who can make a double-sided board, if we just knew the
> and where to get the chemistry to plate the holes before etching.Could not agree more. I know the thoery but the practice it's a whole
>
> You DO know, doncha, that the PTH is done FIRST, then "SOLDER-plating" of the
> desired pattern (including through the holes!), and etch LAST,Took me sometime to figure this one out. But it's not solder but
> with chemistry that will etch copper, but NOT "solder".
>
2002-03-02 by adam_seychell
> --- In Homebrew_PCBs@y..., JanRwl@A... wrote:the
> > each! Seems plating-through should be within the realm of us ol'
> > home-brewers who can make a double-sided board, if we just knew
> steps,whole
> > and where to get the chemistry to plate the holes before etching.
> >
>
> Could not agree more. I know the thoery but the practice it's a
> different ball park.holes
>
>
> > You DO know, doncha, that the PTH is done FIRST, then "SOLDER-
> plating" of the
> > desired pattern (including through the holes!), and etch LAST,
> > with chemistry that will etch copper, but NOT "solder".
> >
>
> Took me sometime to figure this one out. But it's not solder but
> tinned. And the process is called pattern plating.
>
> As a homebrewer it is too expensive for me to send boards out to
> make. If I could only find out a simple way to make plated thru
> at home without killing myself. And eyelets and baluns are too timeHi there,
> consuming.
2002-03-03 by j_hallows
> PTHs are possible to do at home but you should be aware that itHey Adam maybe you should write a produre of your method of making
> involves many chemical stages. Although these chemicals are not
> necessary highly toxic they can be a difficult process to control
> and get working properly. So unless you find chemistry fun and
> don't mind getting your hands wet then I its a complete waste of
> time and money trying to implement a PTH workshop at home. I
> have setup the necessary plating and etching tanks to make a tin
> finish pattern plated board and had taken me almost two years.
> The holes are made conductive using a processes similar to
> MacDermid's BLACKHOLE processes where by a conductive carbon
> black layer deposited inside the holes prior to electroplating. If
> you have any questions then feel free to ask.
>
2002-03-03 by Adam Seychell
> > PTHs are possible to do at home but you should be aware that it
> > involves many chemical stages. Although these chemicals are not
> > necessary highly toxic they can be a difficult process to control
> > and get working properly. So unless you find chemistry fun and
> > don't mind getting your hands wet then I its a complete waste of
> > time and money trying to implement a PTH workshop at home. I
> > have setup the necessary plating and etching tanks to make a tin
> > finish pattern plated board and had taken me almost two years.
> > The holes are made conductive using a processes similar to
> > MacDermid's BLACKHOLE processes where by a conductive carbon
> > black layer deposited inside the holes prior to electroplating. If
> > you have any questions then feel free to ask.
> >
>
> Hey Adam maybe you should write a produre of your method of making
> PTH. I would love to know the costs involved and chemistry. I am not
> familar with the BLACKHOLE method. The hardest part is making the
> holes conductive. I know the squeezee method were you squeeze
> conductive ink into the holes. But the ink is very expensive. Also
> the Gallum method but Gallum is hard to find. Is the BLACKHOLE the
> same.
>
> Thanks.
>
> --
> John Hallows
>
>
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2002-03-03 by caveteursus
2002-03-03 by Hans
> Why not use Circuit Works conductive epoxy?ADVERTISEMENT
>
>
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2002-03-03 by j_hallows
--- In Homebrew_PCBs@y..., Adam Seychell <adam_seychell@y...> wrote:
> The BLACKHOLE processes is fast, cheaper and safer to run than
conventional
> electroless copper. This is expected since its aim is to replace the
> electroless copper line in the PCB fabrication plant. The low
toxicity is the
> reason I choose to develop a carbon black processes myself at home.
However
> the chemistry of BLACKHOLE is a trade secret and your not going to
replicate
> the same results at home. BLACKHOLE SP is the latest process from
MacDermid
> and performs many times better than the process explained below. Of
course
> the hobbyist doesn't need the reliability of a multimillion dollar
plant
> producing a hundreds of panels a day. Its taken me about 6 months
of fiddling
> around with carbon black dispersions, conditioning solutions and
circuit
> board material to get a working process suitable for home use.
Basically my
> process can be written down as follows;
>
> 1) drill PCB
> 2) clean copper surface with week solution of detergent/NaOH and
600 emery
> paper.
> 3) rinse well with tap water
> 4) immerse in a "hole wall conditioner" 1 min
> 5) rinse well with with tap water
> 6) immerse in "carbon dispersion" 1 min
> 7) sponge off excess dispersion with sponge, so all holes are fully
empty.
> 8) hot air dry
> 9) repeat steps 4 to 8
> 10) immerse in "activator" for 1 minute
> 11) rinse well with with tap water
> 12) microetch in a conventional non-chloride etching solution
> 13) spray rinse with with tap water to remove all traces of carbon
on copper
> surface.
> 14) air dry (optional)
>
>
> Bath compositions/conditions;
>
> hole wall conditioner:
> 5 to 10 g/l gelatine
> 0.04 to 0.06 g/l CuSO4.5H20 (as a biocide)
> temperature between 26°C and 32°C
> agitation: unnecessary
>
>
> carbon dispersion:
> 2 to 4% (w/w) of non-ionic surfactant based
> conductive carbon black dispersion paste*
> 6 to 10 g/l acetic acid
> room temperature
> agitation: unnecessary
>
>
> activator:
> 1 g/l of dye D&C Green No.5 , C.I 61570.
> room temperature
> agitation: not known
>
> non-chloride etchant:
> 100 to 200 g/l ammonium persulfate
> or
> 1% hydrogen peroxide
> 10% sulfuric acid.
> both baths may be used at room temperature.
>
>
> * The carbon black dispersion paste is FLEXOBRITE BLACK 258/86
manufactured
> by Degussa Coatings & Colorants.
>
> You will have to phone around and get a 500g sample for aqueous
based
> non-ionic surfactant conductive carbon black dispersion. Many of
the colorant
> manufactures will have these. 500g will last you forever. There is
still a
> whole range of information I left out, either because I haven't
worked it out
> yet or I missed it. The D&C Green No5 is available from food, drug
& cosmetic
> dye suppliers, either as a sample or in small volume (1 kg). Good
luck
>
> Adam
2002-03-03 by j_hallows
> Why not use Circuit Works conductive epoxy?I think this product is just for reworking/repairing traces. Also
2002-03-04 by Adam Seychell
> This sounds good. I assume that this is just for hole activation and
> standard electroplating is done next to build up the holes. What is
> the success rate at home? And estimated costs? I don't want to dive
> into something that would be so hard to replicate. Thanks for the
> Info Adam.
>
> --- In Homebrew_PCBs@y..., Adam Seychell <adam_seychell@y...> wrote:
> > The BLACKHOLE processes is fast, cheaper and safer to run than
> conventional
> > electroless copper. This is expected since its aim is to replace the
> > electroless copper line in the PCB fabrication plant. The low
> toxicity is the
> > reason I choose to develop a carbon black processes myself at home.
> However
> > the chemistry of BLACKHOLE is a trade secret and your not going to
> replicate
> > the same results at home. BLACKHOLE SP is the latest process from
> MacDermid
> > and performs many times better than the process explained below. Of
> course
> > the hobbyist doesn't need the reliability of a multimillion dollar
> plant
> > producing a hundreds of panels a day. Its taken me about 6 months
> of fiddling
> > around with carbon black dispersions, conditioning solutions and
> circuit
> > board material to get a working process suitable for home use.
> Basically my
> > process can be written down as follows;
> >
> > 1) drill PCB
> > 2) clean copper surface with week solution of detergent/NaOH and
> 600 emery
> > paper.
> > 3) rinse well with tap water
> > 4) immerse in a "hole wall conditioner" 1 min
> > 5) rinse well with with tap water
> > 6) immerse in "carbon dispersion" 1 min
> > 7) sponge off excess dispersion with sponge, so all holes are fully
> empty.
> > 8) hot air dry
> > 9) repeat steps 4 to 8
> > 10) immerse in "activator" for 1 minute
> > 11) rinse well with with tap water
> > 12) microetch in a conventional non-chloride etching solution
> > 13) spray rinse with with tap water to remove all traces of carbon
> on copper
> > surface.
> > 14) air dry (optional)
> >
> >
> > Bath compositions/conditions;
> >
> > hole wall conditioner:
> > 5 to 10 g/l gelatine
> > 0.04 to 0.06 g/l CuSO4.5H20 (as a biocide)
> > temperature between 26°C and 32°C
> > agitation: unnecessary
> >
> >
> > carbon dispersion:
> > 2 to 4% (w/w) of non-ionic surfactant based
> > conductive carbon black dispersion paste*
> > 6 to 10 g/l acetic acid
> > room temperature
> > agitation: unnecessary
> >
> >
> > activator:
> > 1 g/l of dye D&C Green No.5 , C.I 61570.
> > room temperature
> > agitation: not known
> >
> > non-chloride etchant:
> > 100 to 200 g/l ammonium persulfate
> > or
> > 1% hydrogen peroxide
> > 10% sulfuric acid.
> > both baths may be used at room temperature.
> >
> >
> > * The carbon black dispersion paste is FLEXOBRITE BLACK 258/86
> manufactured
> > by Degussa Coatings & Colorants.
> >
> > You will have to phone around and get a 500g sample for aqueous
> based
> > non-ionic surfactant conductive carbon black dispersion. Many of
> the colorant
> > manufactures will have these. 500g will last you forever. There is
> still a
> > whole range of information I left out, either because I haven't
> worked it out
> > yet or I missed it. The D&C Green No5 is available from food, drug
> & cosmetic
> > dye suppliers, either as a sample or in small volume (1 kg). Good
> luck
> >
> > Adam
>
>
> To unsubscribe from this group, send an email to:
> Homebrew_PCBs-unsubscribe@yahoogroups.com
>
>
>
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2002-03-04 by caveteursus
2002-03-04 by JanRwl@AOL.COM
> Homebrew is great for PROTO's and One-off's, where you would likeExactly! The only things that would make PTH at home "worth it" would be any
> something in a couple of hours, but the personal economics quickly
> get swamped.
2002-03-06 by Adam Seychell
>In a message dated 04-Mar-02 08:15:05 Central Standard Time,any
>j.walton@... writes:
>
>
>> Homebrew is great for PROTO's and One-off's, where you would like
>> something in a couple of hours, but the personal economics quickly
>> get swamped.
>
>
>Exactly! The only things that would make PTH at home "worth it" would be
>one or combination of the following:for
>
>1. The personal "need" to prove "I can DO that!";
>2. A lack of a professional PC-house within 50 miles, that will do PTH
>you, essentially "while you wait";Yes, it simply not worth doing PTH for a hobby. That's why I am selling the
>3. A need to make PTH boards for a top-secret national-defence project that
>must be completed TONIGHT;
>
>
2002-03-06 by j_hallows
> The cost is not the problem since the carbon dispersion should beavailable
> free from one of the large colorant producers. The dye is similarlyenough to
> available. I got 20 kg of dispersion paste for $130 AU. This is
> make about 1000 liters of solution. I've used about 100 grams sofar. The
> cost will be in building or setting up your chemical tanks. Platingcopper is
> easy but trying to plate uniform smooth copper on to your PCB takesa lot
> more effort. I would say the carbon black process is simplerelative to
> copper plating. In other words, if you can get successful copperplating then
> I'm sure the carbon black process will be easy for you. The successrate for
> plating holes is just about perfect, but it has taken me a longtime to get
> at this stage. The guide I described is a good start. The onlyconcern I have
> is that a different carbon black dispersion concentrate may givedifferent
> results.I had a nice long reply to the group, (covering two posts). But it
>
>
> Adam
>
2002-03-06 by j_hallows
> If I had a design with hundreds of boards, or multilayer boards, orI have to admit I tradionally prototype using wirewrap method. I find
> even tens of through-holes on 4 or 5 boards, I think that I could
> find better uses of my time than etching them "homebrew" style.
> Homebrew is great for PROTO's and One-off's, where you would like
> something in a couple of hours, but the personal economics quickly
> get swamped.
2002-03-06 by Adam Seychell
>I was considering saving all my pennies and buying a commerical
>prototype PCB plating machine. They are around the $1000.00 mark,
>(the cost of sending out 20 boards to be made). I can always make my
>money back by making prototypes for others at half the cost but this
>isn't the main reason. But the main problem is making the holes
>conductive in the first place which Adam address. This method seems
>the easiest but major draw back is the experimenting with chemicals
>to get the right ratio.
>
>This is my first plan. My second plan would be to register in a local
>community college PCB manufacturing course and use thier equipment.
>$200.00 for the course and 50 prototypes made. ;) Cheaper I think.
>
>
>
>
>To unsubscribe from this group, send an email to:
>Homebrew_PCBs-unsubscribe@yahoogroups.com
>
>
>
>Your use of Yahoo! Groups is subject to http://docs.yahoo.com/info/terms/
>
>
2002-03-06 by Hans
>ADVERTISEMENT
> I had a nice long reply to the group, (covering two posts). But it
> seems yahoo decided to screw up my message. But the gist was
> the cost of producing prototypes at home or sending away. I am not
> too concern at plating since I am thinking of buying a prototype
> plating machine. I more worried about making the holes conductive.
> Your prodeduce looks appealing.
>
> Lates.
>
>
>
>
>
> Yahoo! Groups Sponsor
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2002-03-07 by Adam Seychell
>--- In Homebrew_PCBs@y..., Adam Seychell <adam_seychell@y...> wrote:First you should worry about how your going to etch. If you decide on
>> The cost is not the problem since the carbon dispersion should be
>available
>> free from one of the large colorant producers. The dye is similarly
>> available. I got 20 kg of dispersion paste for $130 AU. This is
>enough to
>> make about 1000 liters of solution. I've used about 100 grams so
>far. The
>> cost will be in building or setting up your chemical tanks. Plating
>copper is
>> easy but trying to plate uniform smooth copper on to your PCB takes
>a lot
>> more effort. I would say the carbon black process is simple
>relative to
>> copper plating. In other words, if you can get successful copper
>plating then
>> I'm sure the carbon black process will be easy for you. The success
>rate for
>> plating holes is just about perfect, but it has taken me a long
>time to get
>> at this stage. The guide I described is a good start. The only
>concern I have
>> is that a different carbon black dispersion concentrate may give
>different
>> results.
>>
>>
>> Adam
>>
>
>I had a nice long reply to the group, (covering two posts). But it
>seems yahoo decided to screw up my message. But the gist was
>the cost of producing prototypes at home or sending away. I am not
>too concern at plating since I am thinking of buying a prototype
>plating machine. I more worried about making the holes conductive.
>Your prodeduce looks appealing.
>
>Lates.
>
>
2002-03-07 by j_hallows
> I'm afraid it doesn't work like that. Buying a secondhand platingmachine
> ain't going to make you PCBs.I didn't mean second hand. I have been looking at the Prototype
2002-03-07 by j_hallows
> First you should worry about how your going to etch.You read my mine this was my next question.
> If you decide onIf you
> pattern plate then you have choice of tin or tin/lead metal resist.
> choose tin then you must use alkaline ammonia etch. If you choosetin/lead
> then can use sulfuric/peroxide, ammonium persulfate etch, orammonia etch.
> However, I would be wary on having toxic lead plating solutionslaying
> around. For the ammonia etch it can be chloride or sulfate based. Ifcopper cannot
> chloride based then you have major waste problems because the
> be recovered easily (at least what I know) and you will need totreat then
> dump your solution ($$$).This is like ferric chloride?
> the etchant can be electrolytically regenerated although theetching rate
> is much slower than chloride.Please excuse my ignorance. I have a lot zeal and a lot to learn.
>
> PCB fabrication may look simple on a flow chart but when it comes to
> actually making it work its a whole different story.
>
2002-03-07 by Adam Seychell
>--- In Homebrew_PCBs@y..., Adam Seychell <adam_seychell@y...> wrote:By starting off with blank copper cladded board you mean ? then yes.
>> I'm afraid it doesn't work like that. Buying a secondhand plating
>machine
>> ain't going to make you PCBs.
>
>I didn't mean second hand. I have been looking at the Prototype
>plating machines. Like QuickPLATE. But they all seem to use the
>process of squeezing conductive ink into the hole manually. The INK
>in itself is expensive.
>
>BTW: In your process the board is completely coated then plated
>correct? So the board must have a thinner layer of copper to work
>with in the first place or the thickness would be uneven correct?
>
>Lates.
>
>--
>John Hallows
>
2002-03-07 by Adam Seychell
> > First you should worry about how your going to etch.
>
> You read my mine this was my next question.
>
> > If you decide on
> > pattern plate then you have choice of tin or tin/lead metal resist.
> If you
> > choose tin then you must use alkaline ammonia etch. If you choose
> tin/lead
> > then can use sulfuric/peroxide, ammonium persulfate etch, or
> ammonia etch.
>
> Is this the same stuff called Liquid Tin by MG Chemicals and a
> similar prodouct by Datak? Or would these get disolved by the etching
> solution?
>
> > However, I would be wary on having toxic lead plating solutions
> laying
> > around. For the ammonia etch it can be chloride or sulfate based. If
> > chloride based then you have major waste problems because the
> copper cannot
> > be recovered easily (at least what I know) and you will need to
> treat then
> > dump your solution ($$$).
>
> This is like ferric chloride?
>
> If you use sulfate based alkaline ammonia then
> > the etchant can be electrolytically regenerated although the
> etching rate
> > is much slower than chloride.
> >
> > PCB fabrication may look simple on a flow chart but when it comes to
> > actually making it work its a whole different story.
> >
>
> Please excuse my ignorance. I have a lot zeal and a lot to learn.
>
>
> To unsubscribe from this group, send an email to:
> Homebrew_PCBs-unsubscribe@yahoogroups.com
>
>
>
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2002-03-07 by Steve Greenfield
> Here is a good link describing the steps on manufacturing a__________________________________________________
> multilayer
> board (pattern plating).
>
> http://www.pha.jhu.edu/~akeeney/PWB/
>
> some more PCB info can be had at;
>
> http://www.epa.gov/dfe/pubs/pwb/tech_rep/usecluster/pr_toc.htm
2002-04-14 by Alexandre Domingos F. Souza
>Example: Two boards of Two Sided board with through plated holes, LPIIt seems incredible, but in Brazil, boards are A LOT CHEAPER than USA. The same board you are talking about, costs around $20 for 10 boards ($20 all the 10 boards, not $20 each). Incredible. But true.
>mask and silk screen, any size upto 64 square inches. $33.00 (thirty
>three US dollars) per board total cost $66.00 no tooling charges, there
>are a few limitation on drill sizes the smallest is 20 mil. Plus
>freight... Five days turnaround.
>Hans Wedemeyer