On 10/05/2011 6:21 AM, Jim wrote: > > Thanks DJ > Last week I had a 55 oz jar of transparent emerald green etch. Using > this etch was SLLLOW. I added scrap copper and started bubbling. It took > about 10 hours to turn OPAQUE. I continued to bubble for another 24 > hours. Removed the copper and continued bubbling. After 2 days, it was > still OPAQUE. I added 2 oz HCl ... no change ... 1 oz of 27% H2O2 ... it > turned emerald green. With the additional HCL, I added more copper and > started bubbling. It took 8 hours for it to turn OPAQUE. I continued > bubbling for another 4 hours. I removed the copper and continued > bubbling and after 6 hours it turned transparent emerald green. I don't > have an hydrometer. The color is a transparent BRIGHT emerald green no > trouble seeing through the 5 inch diameter jar of etch ... no hint of > OLIVE green. Should I add more copper? ... When Adam says you can't see > through but a few mm, Is that the ready to etch transparent state or the > spent OPAQUE state? > Jim KI6MZ > > On 5/9/2011 11:46 AM, DJ Delorie wrote: > > The only way to know how "strong" your CuCl etchant is, is to use a > > hydrometer. The copper makes the solution more dense, by measuring > > the density you can determine the copper concentration. > > > > See http://members.optusnet.com.au/~eseychell/PCB/etching_CuCl/ > <http://members.optusnet.com.au/%7Eeseychell/PCB/etching_CuCl/> > > for all the details. > > > > Note: my solution looks like the photo at the top of Adam's page. > > > > "Spent" etchant is opaque BROWN. This may look like dark green at first > > because it's mixed, but see Figure 5 on Adam's page. > > > The bright clear green should be ready-to-etch state. Opaque means it's spent state. Here's a great resource on the chemistry behind it with really good pictures: http://members.optusnet.com.au/~eseychell/PCB/etching_CuCl/index.html <http://members.optusnet.com.au/%7Eeseychell/PCB/etching_CuCl/index.html> Andrew [Non-text portions of this message have been removed]
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Re: [Homebrew_PCBs] Re: Oxygen regeneration of CuCl2
2011-05-09 by Andrew Leech
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