My jar of CuCl ?? was transparent emerald green(~55 Oz.). I put some more copper scraps in it and turned on the bubblier. It ran for 2 days. The contents of the jar turned DARK OPAQUE green. I removed the solid copper scraps and started the bubblier again. I ran it 2 days and the contents of the jar was still DARK OPAQUE green. I added 2 Oz of HCL ... no change. I added 1 Oz of 27% H2O2 and the contents of the jar turned transparent emerald green. ... are we there yet ?? Jim KI6MZ On 5/8/2011 4:49 AM, DJ Delorie wrote: > "tda7000"<Tda7000@...> writes: >> So, I just have to keep adding a little hydrogen peroxide to >> reactivate each time I etch until I've etched enough boards to turn it >> dark, and then just bubbling will reactivate it? > Until you've converted it, you still have an HCl/H2O2 etchant. The H2O2 > breaks down over time, and the HCl evaporates, leaving you with just > water. So, if you're doing this over time, the thing to do is mix only > enough HCl/H2O2 etchant for your board-du-jour, and keep adding it to > your etchant tank. Over time, the CuCl builds up, and you need less > HCl/H2O2 for each board, and can start with the CuCl chemistry checks to > see what you need (HCl or H2O2) each time you etch. Also you can keep a > chunk of copper in the etchant when you're not using it, so the excess > HCl/H2O2 doesn't go to waste. A copper plumbing part will do, like an > elbow. Just remember to take it out before adding the new etchant ;-) > > Remember, the etch does Cu + Cl => CuCl, so you have to have free Cl in > the etchant also! H2O2 alone is not enough. > > > ------------------------------------ > > Be sure to visit the group home and check for new Links, Files, and Photos: > http://groups.yahoo.com/group/Homebrew_PCBsYahoo! Groups Links > > > > > __________ Information from ESET Smart Security, version of virus signature database 6105 (20110508) __________ > > The message was checked by ESET Smart Security. > > http://www.eset.com > > > >
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Re: [Homebrew_PCBs] Re: Oxygen regeneration of CuCl2
2011-05-08 by Jim
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