On 11/11/10 01:31, DJ Delorie wrote: > The usual recipies are designed for one part 37% acid and two parts 2% > peroxide. Since you're using a weaker acid and a stronger peroxide, > you'll have to figure out the new ratios, but it will probably end up > being two parts acid to one part peroxide. That suits me fine -- it's easier to get the acid in large quantities than the peroxide. > Never add peroxide to acid! > Always add acid to peroxide. Yep, I've heard the old saying: "Add acid to water, just like you ought to!" Acid + water is an exothermic reaction, just like mixing FeCl3 granules. Throw water into acid and you get localised boiling, fizzing and hot steam... not really a good thing when dealing with corrosive substances. > If you want to skip right to CuCl, I found that about half a pound of > copper converts 3 liters of CuCl etchant. So just chuck 1lb of copper pipe into the tank, and leave it with the air pump running? You mention that the peroxide degrades in about a week, am I right in thinking this only applies to the HCl+H2O2 etchant, i.e. by the time it's CuCl, this is of little effect? Do sealed bottles of peroxide degrade in the same way, or just open bottles? I suspect I'll probably buy enough peroxide for two attempts, i.e. 2-litre tank, 3 parts chem = 660ml a time, or 1.2l peroxide, and a 5-litre bottle of brick cleaner (about the cheapest way to buy it). Just in case I screw something up...! Thanks, -- Phil. ygroups@... http://www.philpem.me.uk/
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Re: [Homebrew_PCBs] Starting off a HCl+H2O2 / CuCl etch bath
2010-11-11 by Philip Pemberton
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