Why not simply go with using H2O2 (pharmacy grade ~3%) and HCl (available from the HW store in gallon jugs for ~2.50/gallon) Mixed on the spot, and used sparingly, I've etched VERY successfully several times now using a TTF method... <shrug> Ferric Chloride is just a pain to deal with... Hate the stuff... I've also got no other use for FeCl... H2O2, I use fairly often... HCl/Muriatic Acid has uses around the house as well... I can't think of a useful thing I can do with FeCl, other than stain everything in sight... :-) Best! -jw --- In Homebrew_PCBs@yahoogroups.com, "fenrir_co" <fenrir@...> wrote: > > --- In Homebrew_PCBs@yahoogroups.com, Robert Hedan <robert.hedan@> > wrote: > > > > Ok, > > > > > > So I googled and found this link: > > http://www.qsl.net/iz7ath/web/02_brew/14_howto/02_clor/index.htm > > > > This guy regenerates ferric chloride, but that contradicts this link > > from > > the muriatic acid thread: > > http://www.smallsolar.org/workshop/etchant/index.htm > > > > - Copper Chloride has one important benefit that the other commonly > > used > > etchant chemicals (Ferric Chloride and Ammonium Persulphate) don't > > have: > > when it "wears out" it can be regenerated. > > > > So, before I nuke my back yard, can I regenerate ferric chloride? > > And if > > so, what would be a 'relatively' safe procedure? > > > > Robert > > :) > > > > I regenerated Ferric Chloride with just muriatic acid at first. The > result didn't etch as fast as new etchant, but worked. Eventually, > however, I found that beauty supply strength H2O2 (40 Volume = 12% > strength) would regenerate it far better. You can find it at Sally > Beauty Supply if you are in the US, you may have difficulty finding > anything over 20 volume elsewhere, try hairdresser and beauty supply > shops that have hair products. I use about 32 oz per 2 gallons of > etchant, so divide that up to find out how much to use. You should > still add a little acid to keep the pH low. Maybe about a half a cup > to a cup. I don't measure in much detail. > > Using the H2O2 will produce a LOT of foam and some heat, so make sure > the etchant is in a sturdy container (I use a 5 gal bucket inside > another 5 gal bucket) and don't add it too fast or it will 'boil > over'. The resulting etchant works faster than fresh etchant from > Radio Shack. >
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Re: Regenerating Ferric Chloride
2006-07-02 by JW
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