Hi Adam- I was not feeling mislead, I just did not know what to expect. The copper has only been in the acid for 18 hours. The acid still looks clear, as it did when I poured it into the water. The copper in the air looks much as it did at the time of my last post. I hadn't measured the room temperature when I wrote the above, so I went and did this. The etchant temperature is about 65 deg. F. As I measured the temperature, before my very eyes on several spots on the exposed copper wire a turquoise blue coating appeared. That was quite amazing! So I have every reason to believe that things will unfold as they have for you. The tank has been covered with its cover, which has a 9/16" hole in it. Does this process need lots of air exposure at first? Or was it just coincidence that when I took the lid off to take the temperature the process evidenced itself? I did put the entire 1.8 kg of copper in at the start. Thanks for your continuing advice, information, and encouragement. I will keep the list posted about the progress of the etchant. Grant --- In Homebrew_PCBs@yahoogroups.com, Adam Seychell <adam_seychell@y...> wrote: > You should put full 1.8kg of the wire in. I takes about 24 hours > for the acid to really start going dark and cuprous/cupric > chloride mix to be produced. The copper in the air should > eventually go bright blue Cu(OH)2 coating. > Has the HCl still changed from its normal pale yellow to a dark > brown ?. If so then its working. This reaction is an accelerating > one. > I'm sorry if I misguided you and you feel its not working as > expected. I've made 2 batches so far, using this technique. > Eventually I would like to write a web page giving much more > accurate information than I have done so in these posts, > including pictures. I'm still experimenting myself at this stage. > > Just add concentrated acid from now on, there should be enough > water for the moment. Don't hesitate to ask any questions. > > Adam
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Re: Starting CuCl etchant from scratch
2003-04-14 by grantfair2001
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