Stefan Trethan wrote: > On Tue, 06 Sep 2005 05:46:55 +0200, Adam Seychell > <a_seychell@...> wrote: > > >>Dull green is ok, only when it becomes brown is the problem. If you >>dilute a bit of it and it turns bright green then its pretty much >>regenerated. But, this doesn't necessarily mean it'll etch ok. >>I here a lot of people on this group that cannot get air re-generated >>cupric chloride to work, simply because they run their solutions too >>damn week. I have done a side by side comparison with fresh full >>strength ferric chloride (sp.gr 1.47), under exact same conditions and >>the cupric chloride (without any H2O2, ever) is only fractionally slower >>(7.5 minutes for FeCl and 9 minutes for CuCl for bubble etching, 35um >>thick copper at 15\ufffdC). >>Adam > > > > i agree, you need a strong solution to do air-regeneration. > For H2O2, anything works, but as it grows denser the time between H2O2 > applications can be extended, wile at the beginning with a very weak > solution you need to add it each time you etch, at least. Density, and a > enough volume, are the key to air regeneration i think. > > Yes, the more copper the faster, and the more acid the faster. You are only limited by solubility, and HCl fuming. A good compromise I found is to run at sp.gr 1.38~1.45 and acid at 2~3 Molar. This will be almost fast as fresh undiluted ferric chloride. Unfortunately you have to invest in a hydrometer, and perform titration (using a 1 ml syringe) to determine acid concentration about every 20~30 PCBs or so etched. Adam
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Re: [Homebrew_PCBs] Re: Regenerating CuCl
2005-09-06 by Adam Seychell
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