I may not have all the specifics right - it was about 6 months ago but I did add 50 mL of 30% HCl and then aerated. It stayed a dull green, even after a week of aerating. 50 mL of 35% H2O2 brightened it to emerald green and I was able to etch a board with it. Total volume was 2L + 100 mL. I'm sure I was doing something wrong but I just wanted to etch boards not fiddle f*rt around with chemicals. I love AP. Its clear, clean, fast, reliable and very easy to use. Never had to fuss with it. It just works. I still have 2.1 L of mystery etchant if some one wants it... heh heh heh --- In Homebrew_PCBs@yahoogroups.com, Adam Seychell <a_seychell@y...> wrote: > Are you sure you added enough acid *before* aerating ? How do you know > what the acid concentration was after aerating ? > > I find it hard to believe it wouldn't oxidize in that time. > I assume you are looking for the transparent green color to determine if > the bath regeneration was completed. > > Adam > > Phil wrote: > > I tried to use CuCl over a period of 4 months. I was never able to > > regenerate it using a bubbler - even left it running for a week once. > > I added more acid but no regen. However, adding H2O2 made a huge > > difference. My bubbles were fairly small so I think I was getting O2 > > into it. I suspect there is more to it than just pumping oxygen into > > the solution. > > > > --- In Homebrew_PCBs@yahoogroups.com, "stan4312" <stanman@t...> wrote: > > > >>I'm attempting to bootstrap my first batch of CuCl as I type, so > >>this page is fresh off my bookmarks: > >>http://pacificsun.ca/~robert/pcb/cucl.htm Pretty good > >>page on CuCl. Lots of precision chemistry. > >> > >>I thought he also had the following seat-of-the-pants advice: if it > >>hasn't regenerated overnight, add more acid, but glancing back, I > >>see it must have been from somewhere else. > >> > >>Stan > >> > >>--- In Homebrew_PCBs@yahoogroups.com, "johnwhitneyfiat" > >><johnwhitneyfiat@y...> wrote: > >> > >>>I have been off the group for a while and I'm sure this was > >> > >>covered. > >> > >>>In the direction for making etchant from Hydrogen Peroxide and > >> > >>Muratic > >> > >>>Acid, it says that you can regenerate with a bubbler. How long > >> > >>does > >> > >>>this take? I know it will depend on the amount and the area that > >> > >>was > >> > >>>etched, but is there a rule of thumb to make it work. I do have to > >> > >>day > >> > >>>that I make a small bathch and it worked great on a sample board. > >>> > >>>John Whitney > >>>Wis X 1/9 > > > > > > > > > > > > > > Be sure to visit the group home and check for new Links, Files, and Photos: > > http://groups.yahoo.com/group/Homebrew_PCBs > > > > If Files or Photos are running short of space, post them here: > > http://groups.yahoo.com/group/Homebrew_PCBs_Archives/ > > Yahoo! Groups Links > > > > > > > > > > > > > > > >
Message
Re: Regenerating CuCl
2005-09-06 by Phil
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