Are you sure you added enough acid *before* aerating ? How do you know what the acid concentration was after aerating ? I find it hard to believe it wouldn't oxidize in that time. I assume you are looking for the transparent green color to determine if the bath regeneration was completed. Adam Phil wrote: > I tried to use CuCl over a period of 4 months. I was never able to > regenerate it using a bubbler - even left it running for a week once. > I added more acid but no regen. However, adding H2O2 made a huge > difference. My bubbles were fairly small so I think I was getting O2 > into it. I suspect there is more to it than just pumping oxygen into > the solution. > > --- In Homebrew_PCBs@yahoogroups.com, "stan4312" <stanman@t...> wrote: > >>I'm attempting to bootstrap my first batch of CuCl as I type, so >>this page is fresh off my bookmarks: >>http://pacificsun.ca/~robert/pcb/cucl.htm Pretty good >>page on CuCl. Lots of precision chemistry. >> >>I thought he also had the following seat-of-the-pants advice: if it >>hasn't regenerated overnight, add more acid, but glancing back, I >>see it must have been from somewhere else. >> >>Stan >> >>--- In Homebrew_PCBs@yahoogroups.com, "johnwhitneyfiat" >><johnwhitneyfiat@y...> wrote: >> >>>I have been off the group for a while and I'm sure this was >> >>covered. >> >>>In the direction for making etchant from Hydrogen Peroxide and >> >>Muratic >> >>>Acid, it says that you can regenerate with a bubbler. How long >> >>does >> >>>this take? I know it will depend on the amount and the area that >> >>was >> >>>etched, but is there a rule of thumb to make it work. I do have to >> >>day >> >>>that I make a small bathch and it worked great on a sample board. >>> >>>John Whitney >>>Wis X 1/9 > > > > > > > Be sure to visit the group home and check for new Links, Files, and Photos: > http://groups.yahoo.com/group/Homebrew_PCBs > > If Files or Photos are running short of space, post them here: > http://groups.yahoo.com/group/Homebrew_PCBs_Archives/ > Yahoo! Groups Links > > > > > > > >
Message
Re: [Homebrew_PCBs] Re: Regenerating CuCl
2005-09-06 by Adam Seychell
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