Thanks for your input. Hydrogen peroxide is an excellent idea to
start the production of CuCl2. The dark brown color your seeing
that doesn't go away with aeration is because there are too many
Cl(-) ions in solution (too high concentration of HCl). In such
cases, diluting with water will turn the CuCl2 complex from dark
brown/black to green, assuming there is no more CuCl remaining
after the aeration period. How long did you bubble to solution?
It can take many hours. You of course need a cover on the tank
because the bubbles make tiny splashes.
Adam
luther m stroud wrote:
> I prefer the cucl be made with dilute hcl and scap copper and hyrogen
> peroxide 3% from the drug store. start off slow speeds up as th copper
> ions make a green solution if the ecthant turns muddy color from use
> the peroxide returns it to bright green . air bubbles cause splatter and
> cool the solution. i didnt have any luck with air bubbles converting
> from muddy to bright green , peroxide is instant. in an australia
> electronics mag.
> it was sugested to attach a carbon rod with insulated wire ot the etching
> board and place in contact with the solution claimed to increase the
> speed of etch. i havent tried it out yet . what if using a battery the
> pc board positive and scap copper negative rejuvinating the etchant as
> you etch your board. a hygrometer is a weight in a tube of air with a
> calibrated scale submerged partly maybe you can inprovise something. just
> some comments to stimulate experimentation thanks luther
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